Method for measuring and controlling the oxygen concentration in

Chemistry: analytical and immunological testing – Condition responsive control

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73DIG9, 117 15, 117202, 422 62, 436 75, 436138, G01N 3320, G01N 2726, G01N 27411

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active

057233373

ABSTRACT:
A method for measuring and controlling the oxygen concentration in silicon melts which are contained in a silica glass crucible or which can be touched by a silica glass surface can especially be used for achieving a defined, uniform axial and radial oxygen concentration in a growing silicon crystal. The measurement of the oxygen concentration is realized by an electrochemical solid ionic sensor dipped into the melt; the voltage is measured between the sensor and the growing silicon crystal. The oxygen concentration in the melt is controlled by applying a voltage between crystal and silica glass crucible. The apparatus for putting the method into practice includes an electrochemical solid ionic sensor formed of a silica glass tube which encloses a metal/metal oxide mixture, contacted by a metal wire.

REFERENCES:
patent: 4007106 (1977-02-01), Hone et al.
patent: 4330359 (1982-05-01), Shlichta
patent: 4400232 (1983-08-01), Ownby et al.
patent: 4496424 (1985-01-01), Terashima et al.
patent: 5041186 (1991-08-01), Nishio et al.
Willard et al. Instrumetal Methods of Analysis Sixth Edition, Wadsworth Publishing (Belmont CA) 1981, pp. 640-645.

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