Method for manufacturing transition metal boride power

Chemistry of inorganic compounds – Boron or compound thereof – Binary compound

Reexamination Certificate

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C423S289000, C423S295000

Reexamination Certificate

active

07541013

ABSTRACT:
The present invention relates to a method for manufacturing a transition metal boride powder. The method for manufacturing a transition metal boride powder includes: i) manufacturing a mixed powder by mixing a transition metal halogenide powder and an alkali metal borohydride powder; ii) charging the mixed powder and a plurality of balls into a reaction vessel; iii) charging an inert gas into the reaction vessel and sealing the reaction vessel; iv) high energy ball milling the mixed powder and manufacturing a composite powder containing a transition metal boride and an alkali metal halogenide; v) washing the composite powder in water, dissolving the alkali metal halogenide in the water and filtering the transition metal borides; and vi) drying the filtered transition metal boride and collecting the transition metal boride powder.

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patent: 2006/0194695 (2006-08-01), Au
patent: 1096901 (1985-09-01), None
Kudaka et al. Mechanochemical syntheses of Titanium Carbide, diboride and Nitride; Journal of the Ceramic Society of Japan; 107, 11 pp. 109-1024; 1999.
Shi et al.; A Convenient Solid-State Reaction Route to Nanocrystalline TiB2; InorganicChemistry Communications; 7, pp. 192-194; 2004.
Derwent Abstract of SU 1096901 A.
Sasaki et al. Synthesis of Titanium Carbide an Titanium Diboride by Mechanochemical Displacement Reaction; Journal of Materials Science Letters; 20, pp. 1619-1622; 2001.

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