Method for manufacturing monodisperse vaterite type calcium carb

Details Method for manufacturing monodisperse vaterite type calcium carb Method for manufacturing monodisperse vaterite type calcium carb

1993-10-19

1996-02-27

Lewis, Michael

Chemistry of inorganic compounds

Carbon or compound thereof

Oxygen containing

C01F 524

Patent

active

054946514

ABSTRACT:
A monodisperse spherical, ellipsoidal or plate-like vaterite calcium carbonate almost free from secondary aggregation is disclosed. The vaterite type calcium carbonate is prepared by the steps of adding 5-20 times mol equivalent of water with respect to unslaked lime to a methanol suspension of 0.5-12 weight % of unslaked lime and/or slaked lime (in case of slaked, conversion is to be made into unslaked lime of the same mol) to prepare of a mixture of methanol, unslaked lime and/or slaked lime and water, letting carbon dioxide gas through said mixture, adjusting the temperature in the carbonation reaction system to not less than 30.degree. C. before arrival of conductivity within carbonation reaction system at the maximal point on conductivity variation curve in the carbonation reaction system and adjusting the time from start of carbonation reaction to the point where the conductivity is 100 .mu.S/cm to be less than 1,000 minutes. A method for growing or controlling in shape the vaterite calcium carbonate used as matrix is also disclosed.

REFERENCES:
patent: 3321269 (1967-05-01), Yasui et al.
patent: 4732748 (1988-03-01), Stewart et al.
patent: 4767464 (1988-08-01), Strauch et al.
patent: 4793985 (1988-12-01), Price et al.
patent: 4835195 (1989-05-01), Rayfield et al.
patent: 5275651 (1994-01-01), Minayoshi et al.

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