Method for manufacturing metal oxide hollow nanoparticles...

Chemistry of inorganic compounds – Oxygen or compound thereof – Metal containing

Reexamination Certificate

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C423S236000, C044S362000, C977S733000, C977S775000

Reexamination Certificate

active

08052958

ABSTRACT:
Provided is a method for manufacturing a metal oxide hollow nanoparticles with excellent properties more easily and simply by a chemical vapor condensation employing metal β-diketonates as precursors, and a metal oxide hollow nanoparticles manufactured by the method. The method includes: preparing metal β-diketonate as a precursor; evaporating the metal β-diketonate at a predetermined temperature higher than a melting point of the metal β-diketonate; transferring the evaporated metal β-diketonate into a reaction region; thermally decomposing the transferred gaseous metal β-diketonate and simultaneously inducing a reaction of the transferred gaseous metal β-diketonate with oxygen to synthesize the metal oxide hollow nanoparticle; and condensing and collecting the synthesized metal oxide hollow nanoparticles.

REFERENCES:
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Chang et al. Nanostructure ceramics synthesized by chemical vapor condensation. Nanostructured Materials, vol. 6, pp. 321-324, 1995.
Jensen et al. “Preparation of ZnO—Al2O3 particle in a premixed flame”. Journal of Nanoparticle Research 2: 363-373, 2000.
Yadong et al. “Formation of hollow nanocrystals through the nanoscale Kirkendall effect”. Science 304: 711-714, 2004.
Chang et al. “Nanostructured ceramics synthesized by chemical vapor condensation”. Nanostructured Materials, vol. 6, pp. 321-324, 1995.
Lee, Jai-Sung, et al. “Hollow Nanoparticles of Iron Oxide Synthesized By Chemical Vapor Condensation,” Journal of Nanoparticle Research (2004), 6:627-631 DPI: 10.1007/sl 1051-004-6322-8.
Nasibulin et al.,J. Aerosol. Sci., 31(Suppl. 1):S913-S914 (2000).

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