Method for manufacturing fine lead titanate powders

Details Method for manufacturing fine lead titanate powders Method for manufacturing fine lead titanate powders

1987-06-24

1989-03-07

Stoll, Robert L.

Chemistry of inorganic compounds

Oxygen or compound thereof

Metal containing

423619, C01G 2300, C01G 2100

Patent

active

048104841

ABSTRACT:
A method for manufacturing fine powders of lead titanate which includes the steps of reacting a water-soluble titanium compound or the hydrolysis product of a titanium compound with a lead compound in an aqueous alkaline solution having a pH value not less than 11.2, at a temperature not less than 100.degree. C. to obtain a precipitate of lead titanate fine powder, and then recovering the lead titanate fine powder from the remaining solution.
By adjusting the pH and the synthesis temperature at proper values, it is possible to synthesize different forms of lead titanate, including a perovskite structure, a pyrochlore structure, or acicular (needle-like) crystals with a novel crystal phase.
The acicular fine lead titanate crystals have an X-ray diffraction peak at 2.theta.=30.71.degree. using a copper target.

REFERENCES:
patent: 3361519 (1968-01-01), Aykan
patent: 4061583 (1977-12-01), Murata et al.
patent: 4282200 (1981-08-01), Nishikawa et al.

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