Method for making Mo.sub.4 S.sub.4 L.sub.6 (C-2386)

Details Method for making Mo.sub.4 S.sub.4 L.sub.6 (C-2386) Method for making Mo.sub.4 S.sub.4 L.sub.6 (C-2386)

1991-05-24

1992-05-05

Dees, Jose G.

Organic compounds -- part of the class 532-570 series

Organic compounds

Heavy metal containing

556 14, 556 15, 556 28, 556 31, 556 57, C07F 1100

Patent

active

051109638

ABSTRACT:
The present invention is predicated on the discovery that Mo(III) containing compounds will react with salts of a 1,1-dithioacid to form Mo.sub.4 S.sub.4 L.sub.6. Accordingly, there is provided a method for preparing compounds of the formula Mo.sub.4 S.sub.4 L.sub.6 wherein L is a 1,1-dithioacid ligand comprising:

REFERENCES:
patent: 4730064 (1988-03-01), Halbert et al.
patent: 4990271 (1991-02-01), Francis
Kathirgamanathan et al., J. Chem Soc. Chem. Commun., pp. 953-954, 1437-1439 (1985).

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