Method for inhibiting epichlorohydrin fouling

Distillation: processes – separatory – Addition of material to distilland to inhibit or prevent... – For inhibiting or preventing a polymerization reaction

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203 28, 203 65, 203 66, 203DIG6, 203DIG23, 549514, 549541, B01D 334

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049448471

ABSTRACT:
A method of inhibiting fouling in distillation towers, overhead lines, reflux lines, and condensers operating in a process to manufacture and purify epichlorohydrin. This method resides in treating process streams entering or exiting such towers, lines and condensers, including feed streams, reflux streams, gaseous or liquid overhead streams, with an effective antifouling amount of a C.sub.3 -C.sub.9 linear or branched alkyl substituted catechol, or mixtures thereof.

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Khim. Prom. 49,824 (1973), A Continuous Method of Producing Epichlorhydrin, Kyasimov et al.
Kinet, Katal 17 (2), Mokrousva et al., 515 (1976).
L. A. Oshin et al: Neftekhimija (USSR), 15, 281 (1975).

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