Method for infusibilizing pitch fibers

Chemistry of inorganic compounds – Carbon or compound thereof – Elemental carbon

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4234471, 4234472, 4234476, 264 292, D01F 912

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049884921

ABSTRACT:
This invention provides a method for infusibilization of pitch fibers for production of carbon fibers which comprises putting pitch fibers prepared by melt spinning from a spinning pitch in containers, introducing in succession the containers containing the pitch fibers into an infusibilizing furnace divided into a plurality of sections and passing the containers therethrough from inlet to outlet wherein the containers containing the pitch fibers are intermittently moved through the infusiblizing furnace to retain each of the containers in respective sections for a given period of time, during which temperature of respective sections is independently raised from minimum controlled temperature to maximum controlled temperature and thereafter is lowered to the minimum controlled temperature and then the container is moved.

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Hawthorne et al., "High Strength High Modulus Graphite Fibres From Pitch", Nature, vol. 223, Aug. 29, 1970, pp. 946-947.
Patent Abstracts of Japan, vol. 9, No. 134 (C-285) [1857], Jun. 8, 1985.

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