Method for improve x-ray diffraction determinations of residual

X-ray or gamma ray systems or devices – Specific application – Diffraction – reflection – or scattering analysis

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378 71, 428328, 252961, 10628718, G01N 2320

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active

049187112

ABSTRACT:
A process for improving the technique of measuring residual stress by x-ray diffraction in pieces of nickel-base alloys which comprises covering part of a predetermined area of the surface of a nickel-base alloy with a dispersion, exposing the covered and uncovered portions of the surface of the alloy to x-rays by way of an x-ray diffractometry apparatus, making x-ray diffraction determinations of the exposed surface, and measuring the residual stress in the alloy based on these determinations. The dispersion is opaque to x-rays and serves a dual purpose since it masks off unsatisfactory signals such that only a small portion of the surface is measured, and it supplies an internal standard by providing diffractogram peaks comparable to the peaks of the nickel alloy so that the alloy peaks can be very accurately located regardless of any sources of error external to the sample.

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"Preparation of Reference Standards for the X-Ray Spectral Analysis of Powdered Materials" by Shestakov et al., Translated from Zavodskayu Laboratoriya, vol. 41, pp. 948-950, 8/1975.

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