Method for forming Fe-B-R-T alloy powder by hydrogen decrepitati

Metal treatment – Process of modifying or maintaining internal physical... – Magnetic materials

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148103, 148104, 148105, 419 12, 419 33, 419 38, 241 18, 241 24, 241 29, H01F 102

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051435608

ABSTRACT:
A method for the high volume manufacture of Fe-B-R-T alloy powders without sacrificing the resultant magnetic properties (such as intrinsic magnetic coercivity) of the alloy involves hydrogen decrepitation of vacuum cast or die-upset billets of the alloy. Hydriding is carried out at a partial pressure of hydrogen of between 250 and 760 mm Hg at 100.degree. to 500.degree. C. for 30 minutes to 6 hours or longer, depending upon load size. Dehydriding occurs in a vacuum below 10.sup.-2 mm Hg or in an inert atmosphere possessing a partial pressure of hydrogen below 10.sup.-2 mm Hg. The alloy powder is preferably incorporated in matrix or composite magnets by the addition of a binder prior to pressing and orienting. The binder may set during pressing in a hot die, or by heating after pressing in a cold die.

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