Method for forming a non-hygroscopic zinc-phosphate compound and

Glass manufacturing – Processes – Fining or homogenizing molten glass

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651359, 65 85, 423305, 423309, 423314, 501 48, 501 76, C03B 516, C01B 1516, C01B 2526, C03C 317

Patent

active

054825261

ABSTRACT:
The instant invention describes a method for preparing a stable, anhydrous non-hygroscopic zinc phosphate compound which is suitable for use as a batch material in the preparation of zinc-phosphate glasses. This method comprises three basic steps: first, forming an aqueous slurry mixture by intimately mixing a mixture containing phosphoric acid and a zinc-containing compound whereby the so-formed slurry mixture is comprised of a mixture of zinc hydrogen phosphates and exhibits a P.sub.2 O.sub.5 /ZnO weight ratio range between about 1.2 to 2.0; second, heating the so-formed slurry mixture to a temperature and for a time sufficient to achieve both a removal of a sufficient amount of water and the phase transformation of the zinc hydrogen phosphates resulting in zinc-phosphate material comprised of granular solid mixture of zinc metaphosphates and zinc pyrophosphate and third, cooling the zinc-phosphate material to room temperature.

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