Method for fluorinating coal

Fuel and related compositions – Liquid fuels – Aluminum or heavy metal – other than lead – containing

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260694, C10L 902, C07B 900

Patent

active

040736245

ABSTRACT:
Coal is fluorinated by contact with fluorine gas at low pressure. After pial fluorination, when the reaction rate has slowed, the pressure is slowly increased until fluorination is complete, forming a solid fluorinated coal of approximate composition CF.sub.1.55 H.sub.0.15. The fluorinated coal and a solid distillate resulting from vacuum pyrolysis of the fluorinated coal are useful as an internal standard for mass spectrometric unit mass assignments from about 100 to over 1500.

REFERENCES:
patent: 1899808 (1933-02-01), Kern
patent: 2057486 (1936-10-01), Higgins
patent: 2702306 (1955-02-01), Gall et al.
patent: 2808369 (1957-10-01), Hickey

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