Method for firing ceramic honeycomb bodies

Plastic and nonmetallic article shaping or treating: processes – Outside of mold sintering or vitrifying of shaped inorganic... – Producing article having plural hollow channels

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Details

264656, 264657, 264669, 264670, C04B 35195

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active

060276843

ABSTRACT:
A method of fabricating a cordierite ceramic honeycomb structural body which includes the following steps: formulating a batch of raw materials comprising a mixture of kaolin clay, talc, alumina and other cordierite-forming materials, each included in the batch in an effective amount such that the batch is capable of yielding a fired honeycomb body whose predominant crystal phase is cordierite; intimately blending the raw materials with an effective amount of vehicle and forming aids to impart plastic formability and green strength to the raw materials and to form a plastic mixture; forming the raw materials into a green honeycomb structural body by extrusion and thereafter drying and firing the green honeycomb structural body. The firing of the green honeycomb structural body is accomplished through a four-phase heating process as follows (1) heating the green body to a first temperature ranging between about 750-850.degree. C.; (2) heating to a second temperature ranging between about 1250 to 1350.degree. C.; and finally, (3) to a third temperature of at least 1390.degree. C., and (4) maintaining a temperature of at least 1390 but less than 1420.degree. C., for a period of about 12 to 20 hours. In one embodiment, an oxidizing firing atmosphere, comprising no greater than about 6% O.sub.2, is maintained at firing temperatures above the first temperature. Alternatively, a reducing as opposed to an oxidizing, firing atmosphere, comprising no greater than about 3% CO, is maintained at firing temperatures above the first temperature.

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