Method for fabricating carbon nanotube yarn

Chemistry of inorganic compounds – Carbon or compound thereof – Elemental carbon

Reexamination Certificate

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C423S447100, C423S447300, C428S367000, C977S726000

Reexamination Certificate

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07045108

ABSTRACT:
A method of fabricating a long carbon nanotube yarn includes the following steps: (1) providing a flat and smooth substrate; (2) depositing a catalyst on the substrate; (3) positioning the substrate with the catalyst in a furnace; (4) heating the furnace to a predetermined temperature; (5) supplying a mixture of carbon containing gas and protecting gas into the furnace; (6) controlling a difference between the local temperature of the catalyst and the furnace temperature to be at least 50° C.; (7) controlling the partial pressure of the carbon containing gas to be less than 0.2; (8) growing a number of carbon nanotubes on the substrate such that a carbon nanotube array is formed on the substrate; and (9) drawing out a bundle of carbon nanotubes from the carbon nanotube array such that a carbon nanotube yarn is formed.

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patent: 6957993 (2005-10-01), Jiang et al.
patent: 2003/0161950 (2003-08-01), Ajayan et al.
patent: 2004/0047038 (2004-03-01), Jiang et al.
Vigolo et al. “Macroscopic Fibers and Ribbons of Oriented Carbon Nanotubes” Nov. 17, 2000, Science, vol. 290, pp. 1331-1334.
Cheng et al. “Bulk morphology and diameter distribution of single-walled carbon nanotubes synthesized by catalytic decomposition of hydrocarbons” Jun. 19, 1998, Chemical Physics Letters, vol. 289, pp. 602-610.
Zhu et al. “Direct Synthesis of Long Single-Walled Carbon Nanotube Strands” May 3, 2002, Science, vol. 296, pp. 884-886.
Jiang et al. “Spinning continuous carbon nanotube yarns” Oct. 24, 2002, Nature, vol. 419, p. 801.

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