Method for determining tribological properties of a sample...

Measuring and testing – Surface and cutting edge testing – Roughness

Reexamination Certificate

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Reexamination Certificate

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10524729

ABSTRACT:
A method for examining a surface of a sample is described using an atomic force scanning microscope (AFM) comprising a cantilever with a longitudinal extension along which a measuring tip is disposed, which is selectively arranged relative to the sample surface by a means for driving and whose spatial position is detected using a sensor unit. Vibration excitation is conducted at excitation amplitudes which produce inside the cantilever torsional amplitudes with maximum values which form a largely (substantively) constant plateau value despite increasing excitation amplitudes and the resonance spectra, in a range of maximum values of the torsional amplitudes, a widening of the resonance spectrum which is determinable by a plateau width. The resonance spectra, preferably the plateau value, the plateau width and/or the gradient of the respective resonance spectra are used for examining the sample.

REFERENCES:
patent: 5804708 (1998-09-01), Yamanaka et al.
patent: 5852233 (1998-12-01), Arnold et al.
patent: 6880386 (2005-04-01), Krotil et al.
patent: 43 24 983 (1996-07-01), None
patent: 199 00 114 (2000-08-01), None
Arnold, W. et al.; “Atomic Force Microscopy at Ultrasonic Frequencies”, Proceeding International Conference on Non-Destructive Evaluation and Reliability of Mircro- and Nanomaterial Systems; International Society for Optical Engineering, SPIE, vol. 4703, 2002, pp. 53-64.
Rabe, U. et al.; “Quantitative Determination of Contact Stiffness Using Atomic Force Acoustic Microscopy”, Ultrasonics, vol. 38, 2000, pp. 430-437.
Yamanaka, K. et al.; “Quantitative Material Characterization by Ultrasonic AFM”, Surface and Interface Analysis, vol. 27, 1999, pp. 600-606.
Rabe, U. et al.; “Probing Linear and Non-linear Tip-Sample Interaction Forces by Atomic Force Acoustic Microscopy”, Surface and Interface Analysis, vol. 27, 1999, pp. 386-391.
Rabe, U. et al.; “Evaluation of the Contact Resonance Frequencies in Atomic Force Microscopy as a Method for Surface Characterisation (Invited)”, Ultrasonics, vol. 40, 2002, pp. 49-54.

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