Method for determining the end of devolatilizing in a coke oven

Distillation: processes – thermolytic – With measuring – testing or inspecting

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201 41, 250573, 356436, C10B 4710, G01N 2100

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active

045684243

ABSTRACT:
In the operation of a by-product coke oven, in order to provide a coking cycle that meets an aim push time and also includes a coke soaking period of pre-selected length, the method of obtaining a plurality of liquid catch specimens having condensed therein volatiles from samples of gas withdrawn from the oven; determining a light-transmitting value for such liquid catch specimens for the coke devolatilizing period and for the coke soaking period; determining the end of the devolatilizing period based upon the light-transmitting values so determined; and, if necessary, adjusting the heating rate of the coke oven on subsequent coking cycles. Apparatus for obtaining such liquid catch specimens, and for determining such light-transmitting values is disclosed.

REFERENCES:
patent: 2839963 (1958-06-01), Moss et al.
patent: 3544218 (1970-12-01), Cassidy
patent: 3564272 (1971-02-01), Tadworth et al.
patent: 3597084 (1971-08-01), Pagano
patent: 4003803 (1977-01-01), Schmidt-Balve
patent: 4351701 (1982-09-01), Bauer

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