Method for determining hydrogen mobility as a function of...

Measuring and testing – Gas analysis

Reexamination Certificate

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Reexamination Certificate

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07340937

ABSTRACT:
A method for determining the mobility of hydrogen as a function of temperature in superconducting niobium cavities comprising: 1) heating a cavity under test to remove free hydrogen; 2) introducing hydrogen-3 gas into the cavity; 3) cooling the cavity to allow absorption of hydrogen-3; and 4) measuring the amount of hydrogen-3 by: a) cooling the cavity to about 4° K while flowing a known and regulated amount of inert carrier gas such as argon or helium into the cavity; b) allowing the cavity to warm at a stable rate from 4° K to room temperature as it leaves the chamber; and c) directing the exit gas to an ion chamber radiation detector.

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patent: 5041147 (1991-08-01), Knize et al.
patent: 5961362 (1999-10-01), Chalamala et al.
patent: 6497769 (2002-12-01), Martin
Knobloch, J. et al.,“Enhanced Susceptibility of Nb Cavity Equator Welds to the Hydrogen Related Q-Virus”, Presented at the Workshop on RF Superconductivity, Padova, Italy, 1997, pp. 1-8.
Enderlein, G. et al., “Investigations on Hydrogen Contamination of Superconducting Cavities”, Particle Accelerator Conference, 1991. ‘Accelerator Science and Technology’., Conference Record of the 1991 IEEE, May 6-9, 1991, pp. 2432-2434.
Knobloch, J., “The “Q-Disease” in Superconducting Niobium RF Cavities”, Hydrogen in Materials and Vacuum Systems, First International Workshop on Hydrogen in Materials and Vacuum Systems, AIP Conference Proceedings, vol. 671, 2003, pp. 133-150.

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