Method for decontamination of vessels and other equipment pollut

Cleaning and liquid contact with solids – Processes – Hollow work – internal surface treatment

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134 10, 134 11, 134 18, 134 2219, 134 251, 134 254, 134 39, 134 40, 134 41, 134 42, B08B 308, B08B 310, B08B 908

Patent

active

051547767

ABSTRACT:
The present disclosure is directed to a method and apparatus for removing sludge and reactive metallic deposits, primarily sodium, from a reaction vessel. The process involves circulating under an inert atmosphere a solvent which covers the reactive metal and which solvent removes sludge and other sediments in the vessel including greases, processed salts, etc. Preferably, the process is carried out at a slightly elevated temperature perhaps 120.degree. F. or more. Water or primary alcohols or a mix is added ratably to react with the reactive metal until it is completely removed. The discharge temperature is permitted to increase to perhaps 190.degree. F. and is preferably kept below 245.degree. F. to assure relatively easy handling of the solvent discharge. Recirculation is continued after cooling, sparging, settling to remove impurities picked up in the vessel and recirculation. An apparatus is also disclosed.

REFERENCES:
patent: 4666528 (1987-05-01), Arrington et al.
patent: 4908137 (1990-03-01), Chen et al.

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