Method for controlling reaction temperature

Chemistry of inorganic compounds – Miscellaneous process

Patent

Rate now

  [ 0.00 ] – not rated yet Voters 0   Comments 0

Details

210742, 210752, 210199, C07B 3100, C07B 3300

Patent

active

057701741

ABSTRACT:
Oxidation reactions occurring in a plug flow reactor under conditions approximating supercritical water conditions are controlled by injecting a process stream of water and two reactants in non-stoichiometric proportions into the reactor and causing the process stream to flow through the reactor. Water is injected at one or more points downstream from the inlet to lower the temperature of the process stream and additional reactant injected to re-start the reaction. The quench and re-start process is repeated until substantially all oxidizable material in the process stream has be oxidized.

REFERENCES:
patent: 1988456 (1935-01-01), Lysholm
patent: 2647368 (1953-08-01), Tribbnigg et al.
patent: 2697910 (1954-12-01), Brzozowski
patent: 2767233 (1956-10-01), Mullen, II et al.
patent: 2944396 (1960-07-01), Barton et al.
patent: 3101592 (1963-08-01), Robertson et al.
patent: 3449247 (1969-06-01), Bauer
patent: 3464885 (1969-09-01), Land et al.
patent: 3549314 (1970-12-01), Shah
patent: 3606999 (1971-09-01), Lawless
patent: 3654070 (1972-04-01), Pradt et al.
patent: 3849536 (1974-11-01), Morgan
patent: 3853759 (1974-12-01), Titmas
patent: 3899923 (1975-08-01), Teller
patent: 3900300 (1975-08-01), Lehman
patent: 3912626 (1975-10-01), Ely et al.
patent: 3938972 (1976-02-01), Sugimura
patent: 3978661 (1976-09-01), Cheng
patent: 4017421 (1977-04-01), Othmer
patent: 4141829 (1979-02-01), Thiel et al.
patent: 4215094 (1980-07-01), Inao et al.
patent: 4217218 (1980-08-01), Bauer
patent: 4221577 (1980-09-01), Lowrie
patent: 4229296 (1980-10-01), Wheaton et al.
patent: 4272383 (1981-06-01), McGrew
patent: 4292953 (1981-10-01), Dickinson
patent: 4326957 (1982-04-01), Rosenberg
patent: 4338199 (1982-07-01), Modell
patent: 4370223 (1983-01-01), Bose
patent: 4377066 (1983-03-01), Dickinson
patent: 4378976 (1983-04-01), Rush
patent: 4380960 (1983-04-01), Dickinson
patent: 4384897 (1983-05-01), Brink
patent: 4384959 (1983-05-01), Bauer et al.
patent: 4460628 (1984-07-01), Wheaton et al.
patent: 4488866 (1984-12-01), Schirmer et al.
patent: 4543190 (1985-09-01), Modell
patent: 4564458 (1986-01-01), Burleson
patent: 4593202 (1986-06-01), Dickinson
patent: 4594164 (1986-06-01), Titmas
patent: 4668256 (1987-05-01), Billiet et al.
patent: 4698157 (1987-10-01), Gillot
patent: 4714032 (1987-12-01), Dickinson
patent: 4721575 (1988-01-01), Binning et al.
patent: 4733852 (1988-03-01), Glasgow et al.
patent: 4744909 (1988-05-01), Ferraro et al.
patent: 4774006 (1988-09-01), Kaufmann
patent: 4792408 (1988-12-01), Titmas
patent: 4793153 (1988-12-01), Hembree et al.
patent: 4822394 (1989-04-01), Zeigler et al.
patent: 4822497 (1989-04-01), Hong et al.
patent: 4861484 (1989-08-01), Lichtin et al.
patent: 4861497 (1989-08-01), Welch et al.
patent: 4872890 (1989-10-01), Lamprecht
patent: 4878543 (1989-11-01), Chornet et al.
patent: 4880440 (1989-11-01), Perrin
patent: 4891139 (1990-01-01), Zeigler et al.
patent: 4898107 (1990-02-01), Dickinson
patent: 4936990 (1990-06-01), Brunsell et al.
patent: 4963329 (1990-10-01), Burgess et al.
patent: 4968328 (1990-11-01), Duke
patent: 4983296 (1991-01-01), McMahon et al.
patent: 5009857 (1991-04-01), Hearle
patent: 5011614 (1991-04-01), Gresser et al.
patent: 5053142 (1991-10-01), Sorenson et al.
patent: 5057220 (1991-10-01), Harada et al.
patent: 5057231 (1991-10-01), Mueller et al.
patent: 5075017 (1991-12-01), Hossain et al.
patent: 5106513 (1992-04-01), Hong
patent: 5133877 (1992-07-01), Rofer et al.
patent: 5167930 (1992-12-01), Fassbender
patent: 5183577 (1993-02-01), Lehman
patent: 5192453 (1993-03-01), Keckler et al.
patent: 5221486 (1993-06-01), Fassbender
patent: 5232604 (1993-08-01), Swallow et al.
patent: 5232605 (1993-08-01), Baur et al.
patent: 5240619 (1993-08-01), Copa et al.
patent: 5250193 (1993-10-01), Sawicki et al.
patent: 5252224 (1993-10-01), Modell et al.
patent: 5280701 (1994-01-01), Tolman
patent: 5339621 (1994-08-01), Tolman
patent: 5384051 (1995-01-01), McGinness
patent: 5385214 (1995-01-01), Spurgeon
patent: 5387398 (1995-02-01), Mueggenburg et al.
patent: 5421998 (1995-06-01), Li et al.
Chowdhury et al., "Catalytic Wet Oxidation of Strong Waste Waters", AIChE Symp. 151:71 (1975), pp. 46-58.
Freeman, "Innovative Thermal Hazardous Organic Waste Treatment Processes," Noyes Publications: Park Ridge, New Jersey (1985), pp. 12-33.
Gloyna, "Supercritical Water Oxidation --Deep Well Technology for Toxic Wastewaters and Sludges," Technical Report, The University of Texas at Austin, 1989.
Imamura et al., "Wet Oxidation of Acetic Acid Catalyzed by Co-Bi Complex Oxides," Ind. Eng. Chem. Prod. Res. Dev., 21(4), pp. 570-575 (1982).
Lee et al., "Efficiency of Hydrogen Peroxide and Oxygen in Supercritical Water Oxidation of 2,4-Dichlorophenol and Acetic Acid," The Journal of Supercritical Fluids, 3 pp. 249-255 (1990).
Lu et al., "Selective Particle Deposition in Crossflow Filtration," Sep. Sci. and Technol., 24(7&8), 517-540 (1989).
Mahlman et al., "Cross-Flow Filtration in Physical Chemical Treatment of Municipal Sewage Effluents," Oak Ridge Natl. Lab. Technical Report, EPA/600/2-76/025, Feb. 1976.
Modell et al., "Supercritical Water--Testing Reveals New Process Holds Promise," Solid Wastes Management, Aug. 1982.
Murkes, "Low-shear and High shear Cross-flow Filtration," Filtration and Separation, 23(6), 364-365 (1986).
Murkes et al., Crossflow Filtration: Theory and Practice, John Wiley & Sons: New York, 1988.
Opatken, "Aqueous-Phas Oxidation of Sludge Using the Vertical Reaction Vessel System," EPA/600/2-87/022, Mar. 1987.
Perona et al., "A Pilot Plant for Sewage Treatment by Cross-Flow Filtration," Oak Ridge Natl. Lab. Technical Report ORNL-TM-4659, Oct. 1974.
Shapira et al., "Removal of Heavy Metals and Suspended Solids from Battery Wastewaters: Application of Hydroperm Cross-flow Microfiltration," Gen. Battery Corp. Report EPA/600/2-81-147, Aug. 1981.
Thomason et al., "Supercritical Water Destruction of Aqueous Wastes," Hazardous Waste, 1(4), 453-467 (1984).
Teletzke, "Wet Air Oxidation," Chem. Eng. Prog., 60(1), pp.33-38, Jan. 1964.
Yang et al., "Homogeneous Catalysis in the Oxidation of p-Chlorophenol in Supercritical Water," Ind. Eng. Chem. Res., 27(1), pp. 2009-2014 (1988).
Zimmermann, "New Waste Disposal Process," Chem. Eng., pp. 117-120, Aug., 1985.
Zimmerman et al., "The Zimmerman Process and its Applications in the Pulp and Paper Industry," TAPPI, 43(8), pp. 710-715 (1960).
Keng-Chen Chang et al., "Supercritical water oxidation of acetic acid by potassium permanganate," J. of Hazardous Materials, vol. 32, pp. 001-012 (no date available).
Jacobs et al., "Phase Segregration," Handbook of Separation Process Technology, published by John Wiley & Sons (1987).
Stone & Webster Engineering Corp., "Assessment and Development of an Industrial Wet Oxidation System for Burning Waste and Low Grade Fuels," Final Report, Work Performed Under Contract DE-FC07 881D12711, Prepared for U.S. Department of Energy, Sep. 1989.
Todheide et al., "Das Zweiphasengebiet und die kritische Kurve im System Kohlendioxid -Wasser bis zu Druken von 3500 bar," Zeitschrift fur Physikalischo Chemie Neue Folge, Bd. 37, 8. 387-401 (1963).
Zimmermann et al., "The Zimmerman Process and Its Applications in the Pulp and Paper Industry," TAPPI, 43 (8), pp. 710-715 (1960).
Yoshiaki Harada, "Wet Catalytic Oxidation Process for Wastewater Treatment," Abstract (1991).
Sellchiro Imamura et al., "Wet Oxidation of Ammonia Catalyzed by Cerium-Based Composite Oxides," Ind. Eng. Chem. Prod. Res. Dev., vol. 24, No. 1, pp. 75-80 (1985).
Lei Jin et al, "The Effect of Supercritical Water on the Catalytic Oxidation of 1-4-Dichlorobenzene," presented by AIChE Spring Meeting, Orlando, FL, Mar. 19-23 (1990), Abstract.
Dong-Soo Lee et al., "Efficiency of H.sub.2 O.sub.2 in Supercritical Water Oxidation of 2, 4-Dichlorophenol and Acetic Acid," presented at AIChE Spring Meeting, Orlando, FL, Mar. 18-22 (1990).
Teletzke et al., "Components of Sludge and Its Wet Air Oxidation Products," Journal WPCF, 39 (6):994-1005, 1967.
Conditt and Sievers, "Microanalysis of Reaction products in Sealed Tube Wet Air Oxidations b

LandOfFree

Say what you really think

Search LandOfFree.com for the USA inventors and patents. Rate them and share your experience with other people.

Rating

Method for controlling reaction temperature does not yet have a rating. At this time, there are no reviews or comments for this patent.

If you have personal experience with Method for controlling reaction temperature, we encourage you to share that experience with our LandOfFree.com community. Your opinion is very important and Method for controlling reaction temperature will most certainly appreciate the feedback.

Rate now

     

Profile ID: LFUS-PAI-O-1392378

  Search
All data on this website is collected from public sources. Our data reflects the most accurate information available at the time of publication.