Method for cleaning bomb-reduced uranium derbies

Specialized metallurgical processes – compositions for use therei – Processes – Electrothermic processes

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75 844, C22B 6002

Patent

active

042525640

ABSTRACT:
The concentration of carbon in uranium metal ingots induction cast from derbies prepared by the bomb-reduction of uranium tetrafluoride in the presence of magnesium is effectively reduced to less than 100 ppm by removing residual magnesium fluoride from the surface of the derbies prior to casting. This magnesium fluoride is removed from the derbies by immersing them in an alkali metal salt bath which reacts with and decomposes the magnesium fluoride. A water quenching operation followed by a warm nitric acid bath and a water rinse removes the residual salt and reaction products from the derbies.

REFERENCES:
patent: 3088827 (1963-05-01), Mayoteaux
patent: 3140171 (1964-07-01), Trapp
patent: 3148977 (1964-09-01), Teitel
patent: 3290147 (1966-12-01), Duxbury
patent: 3322679 (1967-05-01), Kamemoto et al.
patent: 3709678 (1973-01-01), Helary et al.
patent: 3850623 (1974-11-01), Sheller
patent: 3985551 (1976-10-01), Powell et al.
Harrington, C. D. et al., Eds. "Uranium Production Technology", pp. 245-270, Van Nostrand Co., Princeton, N.J., 1959.

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