Method for catalytic dimerization of isocyanates

Synthetic resins or natural rubbers -- part of the class 520 ser – Synthetic resins – From reactant having at least one -n=c=x group as well as...

Reexamination Certificate

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C560S355000, C560S358000

Reexamination Certificate

active

10432050

ABSTRACT:
The invention concerns a method for preparing polyisocyanates by cyclodimerization of isocyanate functions borne by initial monomer isocyanates. The invention is characterised in that it comprises steps which consist in: a) providing a reaction medium comprising initial monomer isocyanates, optionally in the presence of a solvent; b) adding to said reaction mixture a (cyclo)dimerization catalyst comprising a compound of the family of super acids; c) heating the reaction medium to a temperature ranging between 0° C. and 300° C., advantageously between 20° C. and 200° C. until the desired rate of transformation is obtained; d) optionally inactivating or eliminating the reaction catalyst; and e) optionally eliminating the unreacted monomer.

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Database WPI, Week 8950, Derwent Publications, Lt.d., London, GB, XP002174350 & JP 01 275616 A (Nov. 6, 1989).
Database WPI, Week 0029, Derwent Publications, Ltd., London, GB XP002174351 & JP 2000 103958 A (Apr. 11, 2000).

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