Method for butt welding cross-linked polyethylene pipes...

Adhesive bonding and miscellaneous chemical manufacture – Methods – Surface bonding and/or assembly therefor

Reexamination Certificate

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C156S304100, C156S308400, C156S309600, C156S304500

Reexamination Certificate

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06524425

ABSTRACT:

BACKGROUND OF THE INVENTION
Field of the Invention
The invention relates to a method for the butt welding of crosslinked polyethylene pipes (PE-X pipes) in order to utilize these pipes in industrial and underground pipeline construction.
High-density polyethylene pipes (HD-PE pipes) are distinguished by outstanding properties. In particular in pipeline construction for gas and water, they are assuming a dominant position. They are flexible, elastic, corrosion-resistant, electrically insulating and can be welded unproblematically. However, owing to their susceptibility to notching and abrasion, they must be laid an ground which is free from stones, possibly requiring a sand fill. It is not uncommon for this sand fill to cost more than the pipe. Therefore, trenchless laying and re-lining by drawing the pipes into existing worn-out pipelines is hot economically possible. These requirements and restrictions ultimately determine the costs of the pipeline construction.
Crosslinked polyethylene pipes (PE-X pipes) even surpass the properties of high-density polyethylene pipes (HD-PE pipes), since their temperature resistance goes up to +100° C., they are resistant to abrasive solids and media, they have good long-term resistance, a low friction coefficient and do not tend toward stress cracking or either slow or fast crack propagation. These positive properties, in particular the relatively high wear resistance and the good long-term resistance of -he PE-X pipes, could be cost-effectively utilized in the public sector for gas, water, sewage and cable pipes. The notch resistance of PE-X pipes means that no laborious and cost intensive sand fill is required any longer and also allows trenchless pipe laying with corresponding deep plowing. Furthermore, it also permits the re-lining of steel drinking water and sewage lines, which are drawn into the flexible and scratch-resistant PE-X pipe. This leads to considerable savings by simplifying the laying technique and to a possible reduction in the pipe wall thickness on account of the greater strength of the PE-X pipes.
However, in the production of pipeline systems, the joining technique constitutes a major problem. Just as the previously mentioned properties of PE-X pipes are advantageous, so the lack of weldability is disadvantageous. The crosslinkage causes the thermoplastic character of the polyethylene starting material to be lost. This means that, among the findings according to the general consensus, crosslinked polyethylene (PE-X) does not enter into an integral bond with itself.
Traditional welding methods lead only to very inadequate weld-seam strengths. Welding methods which are distinguished by high cost-effectiveness in tradicional PE pipeline construction are heating-element welding for pipe diameters >110 mm and electric socket fusion welding (in industrial pipeline construction also heating-element socket fusion welding) mostly for smaller pipe diameters.
Apart from electric socket fusion welding, these welding methods cannot be used for crosslinked PE pipes, since, on account of its molecular structure, crosslinked polyethylene (PE-X) represents a thermoelastic and, under the effect of heat in the welding temperature range for HD-PE, no longer melts but just becomes elastomeric.
Since the mid-1970s, crosslinked polyethylene pipes (PE-X pipes) of up to 63 mm, have been used in the sanitary sector and in age hot-water and heating sector and also for gas pressure lines and compressed-air lines. In the case of these lines, the usually long pipes are connected to one another by means of mechanical connectors of brass or high-grade steel (specialist periodical gwf-Gas-Erdgas, year 131, 1990, issue 10/11, pages 477-482).
The disadvantage of these solutions is the high cost and installation effort, which increases with increasing pipe diameter. In addition, the connectors upset the material-related range of properties of crosslinked polyethylene. The great interest of all pipeline constructors, in particular of the gas and water industries, in utilizing the outstanding. properties of PE-X pipes led to investigations into connection possibilities and the reliability of these connections.
The general consensus was to assume that PE-X cannot be welded. Investigations undertaken by institutes and pipeline construction companies in Germany and elsewhere showed, however, that it is possible to weld crosslinked polyethylene with uncrosslinked polyethylene. It was also established that PE-X cannot be welded with PE-X.
Heating-element welded connections between PE-X and HD-PE pipelines achieved a welding factor of >0.5 (“Einsatz des Rohrwerkstoffes PE-X in der Gasversorgung” [use of the pipe material PE-X for gas supply], Mitgliederinformation [information for members] November 1987 of the Kunststoffrohrverbandes e.V. [German plastic pipe association], Bonn). However, a PE-X pipe/HD-PE pipe connection is of no commercial significance. Furthermore, the use of electric welding sockets made of HD-PE for connecting PE-X pipes was successfully tested. In the welding process, the HD-PE is melted, the PE-X just becomes elastomeric. Strength determinations showed that this connection is suitable for the gas and water supply sector. Some pipelines are in operation (“Der Rohrleitungswerkstoff PE-X; Rohrwerkstoffeigenschaften, Qualitätssicherung und Haupteinsatzgebiete” [the pipeline material PE-X; pipe material properties, quality assurance and main areas of use], of the conference proceedings and address before the 1998 international plastic pipe conference in Wiesbaden on Apr. 27 and 28, 1998 and “Entscheidungskriterien bei der Auswahl von Rohrwerkstoffen in der Gasversorgung” [decision-making criteria in the selection of pipe materials for gas supply], likewise from the cited conference proceedings).
This method of connection with electric welding fittings is cost-intensive as the pipe diameter becomes greater and is not suitable for the re-lining of pipe systems, since the electrical welding sockets get in the way when the PE-X pipe is drawn in.
In the patent literature, DD-WP 139 544, disclosed a method of connecting crosslinked semifinished products, in particular pipes of crosslinked Polyethylene. According to this, the joining faces of the pine ends to be welded are heated with a flat-formed heating element to at least 450° C., with a warming-up time of 8 seconds, and, after removal of the heating element, are joined together under high pressure, the pressure being maintained until the joining zone has cooled to ambient temperature. This method has not been adopted for practical pipeline construction, since no reproducible or satisfactory weld-seam strengths were achieved.
Furthermore, GB-A-2 246 318 discloses a butt-welding method for connecting pipes, fittings, branches and the like of medium—or high-density polyethylene, in which the pipe ends to be connected are heated to welding temperature in a welding device with a plate-shaped heating element, then joined together and left in the welding device until the joining zone has cooled. In the butt welding of pipes of relatively large diameter, a long time is required for the pipe ends to warm up to the welding temperature. This long warming-up time is to be shortened and consequently a time saving in the overall welding process is to be achieved. For this purpose, the butt-welding device is equipped with a heating element (heating plate), which has grooves or a contour profile on both sides, so that the heat transfer from the heating element to the pipe ends is improved by the enlargement of the heating element surface achieved in this way. The profilings may be configured in many ways and have the form of concentric rings or a pyramid structure (waffle iron pattern) or are formed as radial grooves/radial serration. The suitable profile depth is in the range from 1-10 mm.
SUMMARY OF THE INVENTION
The object of the invention is to provide a method for the butt welding of crosslinked polyethylene pipes, preferably for diameters >9

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