Method and device for the sulfonation or sulfation of...

Organic compounds -- part of the class 532-570 series – Organic compounds – Sulfate esters

Reexamination Certificate

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C558S044000, C422S220000

Reexamination Certificate

active

07968742

ABSTRACT:
A method and a device for the sulfonation or the sulfation of organic liquid raw materials with an SO3/air mixture and other reaction gases in order to perform rapid, highly exothermic gas-liquid reactions in conventional thin-layer falling-film reactors are disclosed. The introduction of the SO3/air mixture occurs through several feed locations, which are located within (along) the reaction tube or reaction tubes or in the annular gap of annular-gap falling-film reactors. High peak temperatures, undesirable byproducts, worsening of the color and local oversulfation or oversulfonation, which leads to side reactions, are largely avoided.

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