Method and device for the production of alkylates

Chemistry of hydrocarbon compounds – Saturated compound synthesis – By condensation of a paraffin molecule with an olefin-acting...

Reexamination Certificate

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C585S709000, C585S720000, C422S224000, C422S234000, C422S235000, C210S188000, C210S189000, C210S192000, C210S513000, C210S519000, C210S521000

Reexamination Certificate

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07435864

ABSTRACT:
Disclosed is a device for the production of alkylate(s) by sulfuric acid alkylation of at least one isoparaffin such as isobutane with at least one olefin, such as butylenes. The device includes a mixing chamber for preparing a mixture of the isoparaffin with recycled reaction products. It also includes an emulsion chamber for preparing a first hydrocarbons-in-sulfuric acid emulsion, where the mixture prepared in the mixing chamber is injected in multiple parallel jets into a sulfuric acid composition. The device further includes a pre-reaction chamber for preparing a second emulsion, where a given portion of the olefin is injected in jet streams into the first hydrocarbons-in-sulfuric acid emulsion coming from the emulsion chamber. Last of all, the device includes a reaction chamber of given height and cross-section where the second emulsion coming from the pre-reaction chamber is injected through nozzles and another portion of olefin is injected in jet streams all over the cross-section and height of the reaction chamber. The reaction chamber is devised so that the second emulsion is circulated in a closed circuit and it has an outlet through which a balanced amount of reaction mixture is continuously discharged. All of said mixing chamber, emulsion chamber, pre-reaction chamber and reaction chamber are coaxially arranged one above the other in vertical position and altogether form a reactor with the prechamber being located at the bottom of the reactor and the reaction chamber on top thereof. A method for the production of alkylates by means of the above device is also disclosed.

REFERENCES:
patent: 3175023 (1965-03-01), Gross et al.
patent: 3544652 (1970-12-01), Van Dijk
patent: 5443799 (1995-08-01), Alexanyan et al.
patent: 5777189 (1998-07-01), Alexanyan et al.
patent: WO 95/04019 (1995-02-01), None
patent: WO 99/48845 (1999-09-01), None
Patent Abstract RU 2,131,861, Aug. 3, 1993.
Database WPI, Section Ch, Week 199822, Derwent Publications Ltd., AN 1998-249587, XP002176791, RU 2 092 475, Oct. 10, 1997.

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