Method and composition for forming protective precipitate on...

Earth boring – well treating – and oil field chemistry – Well treating – Contains inorganic component other than water or clay

Reexamination Certificate

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C507S261000, C507S269000

Reexamination Certificate

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07612023

ABSTRACT:
A method and composition for protecting cement surfaces in a well bore treatment zone from the destructive effects of acid mud and other acidization processes commonly used to stimulate hydrocarbon production from the formation, includes contacting the cement with an aqueous acid mixture of HAc and HF in a mutual solvent for a sufficient period of time to form a protective deposit or precipitate layer that is resistant to the acidization composition. In a preferred embodiment, the aqueous acid mixture includes corrosion inhibitors and inhibitor aids, and a preflush with an ammonium chloride solution in a mutual solvent is used to prepare the cement surfaces in the treatment zone.

REFERENCES:
patent: 3402770 (1968-09-01), Messenger
patent: 3601197 (1971-08-01), Ayers et al.
patent: 4737296 (1988-04-01), Watkins
patent: 5508324 (1996-04-01), Cook
patent: 5529125 (1996-06-01), Di Lullo Arias et al.
patent: 2003/0060375 (2003-03-01), Grainger et al.
Sigma-Aldrich data sheet for diethyleneglycol monobutyl ether—2009.

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