Method and apparatus to start-up controlled freezing zone proces

Refrigeration – Processes – Circulating external gas

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62 18, 62 20, 62 28, 62 44, F25J 500

Patent

active

050622706

ABSTRACT:
The invention relates to a method and apparatus for start-up, transformation from start-up to normal operation and normal separation of carbon dioxide and other acid gases from methane using a distillation column with a controlled freezing zone. Normally, the feedstream is treated in at least one distillation zone, a controlled freezing zone, and another acid gas stripping apparatus. The freezing zone produces a carbon dioxide slush which is melted and fed into a distillation section and a methane-enriched stream which is fed to a separate stripping unit. Start-up is accomplished by refluxing the product stream from the separate stripping unit to the distillation column. Transformation is accomplished by separating the methane-enriched stream produced by the freezing zone into a liquid component for refluxing to the column and a vapor component to be fed to the separate stripping unit.

REFERENCES:
patent: 4383841 (1983-05-01), Ryan et al.
patent: 4417909 (1983-11-01), Weltmer et al.
patent: 4462814 (1984-07-01), Holmes et al.
patent: 4533372 (1985-08-01), Valencia et al.
patent: 4636334 (1987-01-01), Skinner et al.
patent: 4761167 (1988-08-01), Nicholas et al.

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