Method and apparatus to make high molecular weight melt...

Synthetic resins or natural rubbers -- part of the class 520 ser – Synthetic resins – From phenol – phenol ether – or inorganic phenolate

Reexamination Certificate

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Details

C264S176100, C264S219000, C528S198000

Reexamination Certificate

active

06887969

ABSTRACT:
Usually, polycarbonate polymerization is limited by the rate at which inhibitory byproducts, such as phenol and salicylate, can be removed from the reaction. To facilitate the removal of volatile reaction byproducts from the reaction as polymerization occurs, the present invention provides a spray mist reactor. The formation of a spray mist polymerization reaction allows for the creation of an enormous surface area for exchange of volatile byproducts. The present invention is applicable to polymerization of polycarbonate and its copolymers starting with monomers or oligomers. The invention may be used to increase throughput and minimize initial investment for a give melt process, especially the fast reacting bis(methylsalicylate) carbonate process.

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patent: WO 9845246 (1998-10-01), None
patent: WO 9947580 (1999-09-01), None
patent: WO 0063274 (2000-10-01), None

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