Method and apparatus for the production of metal oxide powder

Chemistry of inorganic compounds – Oxygen or compound thereof – Metal containing

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423593, 423335, 423339, 423598, 423600, 423604, 423608, 423625, 423636, 204186, 501 1, 501 12, C01B 1314

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active

051223600

ABSTRACT:
The present invention provides a method for preparing metal oxide powder. A first solution, which is substantially organic, is prepared. A second solution, which is an aqueous solution substantially immiscible in the first solution, is prepared and delivered as drops to the first solution. The drops of the second solution are atomized by a pulsed electric field forming micro-drops of the second solution. Reagents in the first solution diffuse into and react with reactants in the micro-drops of the second solution forming metal hydroxide or oxalate particles. The metal hydroxide or metal oxalate particles are then recovered and dried to produce the metal oxide powder. An apparatus for preparing a metal oxide powder is also disclosed.

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Slamovich, et al, "Spherical Zirconia Particles via Electrostatic Atomization . . . " Mat. Res. Soc. Proc. vol. 121, 1988, pp. 257-262.
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Clinton, Sam D., Mass Transfer of Water from Single Aqueous Sol Droplets Fluidized in a Partially Miscible Alcohol, 1972.

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