Method and apparatus for spinning hollow fiber membranes

Plastic and nonmetallic article shaping or treating: processes – Forming continuous or indefinite length work – Shaping by extrusion

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2642093, 26421115, 26421121, 26421123, 26421113, 427245, 2105003, B29C 4788

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active

058716807

ABSTRACT:
A process for the preparation of anisotropic hollow fibers useful as permselective separation membranes and for producing composite membranes thereof, involves extruding a spinning dope through a spinneret that extends into a coagulation chamber maintained at subatmospheric pressure, conveying the nascent hollow fiber through a column that extends into the reduced pressure chamber, and contains at least two different abutting liquids arranged in sequence. An apparatus for conducting the process includes the vacuum chamber, the spinneret and the column that extends into the vacuum chamber and is equipped with entrance and exit ports for introduction and removal of at least two abutting liquid coagulation media.

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Preparation of asymmetric gas separation membranes with high selectivity by a dual-bath coagulation method, Hof, Journal of Membrane Science; 70 (1992), 17-30.
Influence of guench medium on the structures and gas permeation properties of polysulfone membranes made by wet an dry/wet phase inversion, Pinnau.
Journal of Membrane Science, 71 (1992) 81-96; Pore size control technique in the spinning of polysulfone hollow fiber ultrafiltration membranes, Doi, Desalination, 80 (1991), 167-180.

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