Method and apparatus for removal of sodium carbonate from cyanid

Refrigeration – Separator for solidified constituent of liquid mixture

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62384, 62464, 165132, 204274, 204DIG13, 422254, B01D 904, C02F 122

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043654819

ABSTRACT:
The invention is an improved apparatus for the removal of sodium carbonate from cyanide plating baths. The method involves the precipitation of sodium carbonate by the effect of cooling the cyanide plating bath liquid. A container is submerged in the solution with the container opening extending above the plating bath solution level. The container is filled with dry ice and water which produces a temperature of approximately zero degrees centigrade inside of the container. The solution adjacent to the exterior of the container is cooled so that excess sodium carbonate is precipitated as a crystalline deposit. After a desired interval, the container is removed with the encrustation of sodium carbonate for disposal.

REFERENCES:
patent: 1430900 (1922-10-01), Haferkamp
patent: 1943971 (1934-11-01), Hulse
patent: 1980727 (1934-11-01), Hults
patent: 2073664 (1937-03-01), Weisberg et al.
patent: 2186853 (1940-01-01), Yost
patent: 2445294 (1948-07-01), Nelson
patent: 2516105 (1950-07-01), Mateosian
patent: 3737384 (1973-06-01), Fletcher et al.
William Blum et al., "Principles of Electroplating and Electroforming," p. 86, (1949).

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