Method and apparatus for producing particles using...

Plastic and nonmetallic article shaping or treating: processes – Formation of solid particulate material directly from molten...

Reexamination Certificate

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C210S639000, C210S737000, C264S011000, C264S012000, C424S489000

Reexamination Certificate

active

07455797

ABSTRACT:
The present invention provides a method of producing particles via a supercritical fluid processing technique, an apparatus for carrying out the method and the particles produced thereby. The method includes: (1) providing: a supercritical fluid; a first solvent that is soluble in the supercritical fluid; a second solvent that is substantially insoluble in the supercritical fluid and is at least partially soluble in or miscible with the first solvent; and a solute that is soluble in the first solvent and is substantially insoluble in the second solvent and the supercritical fluid; (2) contacting the first solvent, the second solvent and the solute together to form a solution; and (3) contacting the solution with the supercritical fluid to extract the first solvent from the solution and precipitate the solute in the form of particles that are suspended in the second solvent.

REFERENCES:
patent: 5639441 (1997-06-01), Sievers et al.
patent: 6113795 (2000-09-01), Subramaniam et al.
patent: 6184270 (2001-02-01), Beckman et al.
patent: 6372260 (2002-04-01), Andersson et al.
patent: 6998051 (2006-02-01), Chattopadhyay et al.
patent: 7083748 (2006-08-01), Chattopadhyay et al.
Publication: “Introduction to Supercritical Fluids”, Critical Processes Ltd. “www.criticalprocesses.com/SCFmore.html”, adapted from the introduction to Fundamentals of Supercritical Fluids by Tony Clifford, published by the Oxford University Press in 1998.
above publication has es 1-5, downloaded from the Internet on Jul. 5, 2007.
Publication: “Supercritical Fluid—Wikipedia, the free encyclopedia”, “en.wikipedia.org/wiki/Supercritical—fluid”, pp. 1-3, page last modified Jun. 26, 2007, downloaded from the Internet on Jul. 5, 2007.
U.S. Appl. No. 60/445,944, filed on Feb. 7, 2003.

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