Method and apparatus for producing microshells

Plastic and nonmetallic article shaping or treating: processes – Formation of solid particulate material directly from molten...

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65 214, 75331, 75338, 75340, 75342, 264 12, 264 13, 264 15, 425 6, 425 7, B29B 910

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050552406

ABSTRACT:
A method is described for forming hollow particles, or shells, of extremely small size. The shell material is heated to a molten temperature in the presence of a gas that is at least moderately soluble in the shell material, to form a solution of the molten shell material and the soluble gas. The solution is atomized to form a multiplicity of separate droplets that are cooled while in free fall. Cooling of a droplet from the outside traps the dissolved gas and forces it to form a gas bubble at the center of the droplet which now forms a gas-filled shell. The shell is reheated and then cooled in free fall, in an environment having a lower pressure than the gas pressure in the shell. This causes expansion of the shell, to form a shell having a small wall thickness compared to its diameter.

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patent: 4133854 (1979-01-01), Hendricks
patent: 4257799 (1981-03-01), Rosencwaig et al.
patent: 4344787 (1982-08-01), Wang et al.
patent: 4424287 (1984-01-01), Johnson et al.
patent: 4485520 (1984-12-01), Handl et al.

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