Method and apparatus for preparing a dialkyl carbonate

Organic compounds -- part of the class 532-570 series – Organic compounds – Carbonate esters

Reexamination Certificate

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Reexamination Certificate

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06977308

ABSTRACT:
A method of preparing a dialkyl carbonate includes reacting an alkanol, oxygen, carbon monoxide, and a catalyst to form a mixture that includes a dialkyl carbonate and an alkyl chloroformate. The mixture is separated into a liquid fraction and a gaseous fraction, and alkyl chloroformate is removed from the gaseous fraction. Also described is an apparatus for carrying out the method. The method is particularly useful for preventing corrosion in a cold wash unit that removes further organic impurities from the gaseous fraction.

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