Method and apparatus for electrothermal atomization of samples

Optics: measuring and testing – By dispersed light spectroscopy – With sample excitation

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356 36, 356244, G01N 2174

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049813560

ABSTRACT:
Sample liquid is vaporized by a thermospray vaporizer with a heated capillary tube. The end of the capillary tube is inserted into a graphite tube furnace while the furnace and a vertical sample platform in the furnace is at an above-ambient deposition temperature. Vapor spray emerging from the capillary tube is directed at the platform. Sample substances are deposited on the platform while vaporized solvent is drawn off by a vacuum.

REFERENCES:
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patent: 4147434 (1979-04-01), Huber
patent: 4303339 (1981-12-01), Glaser et al.
patent: 4361401 (1982-11-01), Smith, Jr. et al.
patent: 4895443 (1990-01-01), de Loos-Vollebregt et al.
Analytical Instrumentation, vol. 16, No. 2, 1987, pp. 275-280.
Article in Spectrochimica Acta, vol. 33B, 1978, pp. 153-159, "Electrothermal Atomization-The Way Toward Absolute Methods of Atomic Absorption Analysis".
Analytical Chemistry, vol. 54, No. 14, Dec. 1982, pp. 1515A-1516A and 1518A and 1520 A and 1522A and 1524A.
Trends in Analytical Chemistry, vol. 6, No. 7, Aug. 1987, pp. 171-175.
Analytical Chemistry, vol. 55, No. 2, Feb. 1983, pp. 204-208.

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