Material surface treatment method using concurrent...

Electrolysis: processes – compositions used therein – and methods – Electrolytic synthesis – Utilizing electromagnetic wave energy during synthesis

Reexamination Certificate

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C205S341000, C205S687000, C205S704000

Reexamination Certificate

active

07442287

ABSTRACT:
A method of preparing a material surface, such as palladium, to facilitate desirable reactions, especially exothermic reactions in a liquid medium, involves placing the material whose surface is to be treated into an electrolytic cell as at least one of the electrodes and then concurrently stimulating the material electrically, vibrationally and photonically. The electrolytic cell includes a solution in water of an electrolyte, a siliceous surfactant and a pH-adjusting agent, all heated and maintained at or just below its boiling point. A series of voltage pulses are applied to the electrodes over an extended time period while also being illuminated with intensity-modulated light pulses. The material surface thus treated exhibits crater sites and silica coatings, evidencing a change in bonding of the palladium surface, as well as a sustained exothermic reaction.

REFERENCES:
patent: 4167461 (1979-09-01), Dickson et al.
patent: 4790916 (1988-12-01), Murphy et al.
patent: 2005/0199747 (2005-09-01), Roarty
patent: WO2004044923 (2004-05-01), None
C.J. Stephanson et al., “Synthesis of a Novel Anionic Hydride Organosiloxane Presenting Biochemical Properties”, Int'l Assoc. for Hydrogen Energy, 28, 2003, pp. 1243-1250.

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