Synthetic resins or natural rubbers -- part of the class 520 ser – Synthetic resins – From carboxylic acid or derivative thereof
Patent
1985-12-20
1987-03-31
Phynes, Lucille M.
Synthetic resins or natural rubbers -- part of the class 520 ser
Synthetic resins
From carboxylic acid or derivative thereof
528275, 528276, 528277, 528485, 528486, 528489, C08G 6326
Patent
active
046544135
ABSTRACT:
A polybutylene terephthalate is manufactured by the steps of polycondensating in the liquid phase terephthalic acid or a lower alcohol ester thereof as the acid component and 1,4-butanediol as the diol component to obtain a prepolymer of polybutylene terephthalate, solidifying the prepolymer and further polymerizing the prepolymer in the solid phase to obtain a polybutylene terephthalate of a higher polymerization degree, 0.001 to 5 percent by weight, based on the prepolymer, of a nucleator being added to the polymerization mixture at any time during a period of from the monomer-mixing stage before the starting of the solid phase polymerization, the solid phase polymerization being conducted in the presence of the nucleator uniformly dispersed in the polymerization mixture. The solid polymerization can be treated subsequently to the liquid polymerization and can proceed in a short time.
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patent: 4460731 (1984-07-01), Kochanowski et al.
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patent: 4536531 (1985-08-01), Ogawa et al.
Phynes Lucille M.
Polyplastics Co. Ltd.
Sayko Jr. Andrew F.
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