Manufacture of nitric esters

Details Manufacture of nitric esters Manufacture of nitric esters

1962-12-18

1976-12-28

Sebastian, Leland A.

Chemistry of carbon compounds

Miscellaneous organic carbon compounds

C-metal

260466, C07C 7702

Patent

active

040001792

ABSTRACT:
1. A process for the manufacture of a nitric ester by the nitration of an alcohol by a nitrating acid wherein the alcohol and the nitrating acid are reacted together in the presence of an inert highly halogenated hydrocarbon containing fluorine and which is a solvent for and has a boiling point which is between 0.degree. and 50.degree. C and which is below that of the nitric ester product whereby the temperature of the reaction mixture is limited to that of the boiling point of the solvent by evaporation of part of the solvent, separating out the solvent containing dissolved nitric ester from the reaction mixture, and evaporating the solvent to leave the nitric ester.

REFERENCES:
boshman et al., Chem. Reviews, vol. 55, pp. 485 to 488 (1955).

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