Manufacture of alkyl silicates

Organic compounds -- part of the class 532-570 series – Organic compounds – Silicon containing

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C07F 704

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042117178

ABSTRACT:
Ethyl or other lower alkyl silicate is prepared by the direct reaction of alcohol and silicon thereby avoiding the generation of hydrogen chloride as a by-product. The reaction is carried out at elevated temperature in a catalytic solution of high thermal capacity.

REFERENCES:
patent: 2445576 (1948-07-01), Haber
patent: 2569784 (1951-10-01), Smith
patent: 3232972 (1966-02-01), Beanland
patent: 3627807 (1971-12-01), Bleh et al.
patent: 3641077 (1972-02-01), Rochow
patent: 3775457 (1973-11-01), Muraoka et al.

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