Manufacture and consolidation of alloy metal powder billets

Specialized metallurgical processes – compositions for use therei – Compositions – Consolidated metal powder compositions

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72272, 75246, 419 28, 419 31, 419 38, 419 48, 419 53, 419 66, 419 67, G22F 100

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046327029

ABSTRACT:
Metal powder of the desired composition having a particle size of -80 mesh is charged into an extrusion container, preferably a piece of carbon steel pipe, in successive layers about two inches thick. Each layer is compacted after deposition by a high energy rate forming ram so as to raise the tap density of the powder to about 80% of theoretical. An inner cover plate is then placed loosely on the compacted powder in the extrusion container, and is not attached to the container shell. On top of this inner plate is placed an outer cover plate which is welded to the container shell. Both plates are also of carbon steel, but are much thicker than the container wall. The container so prepared is heated in a heating furnace to a temperature below the melting temperature of the container and the powder alloy thus raising the density of the powder to about 90-93% of theoretical. The heated container is rapidly transferred to an extrusion press and hot extruded at a reduction ratio of about 3 to 1 and at a pressure of about 3000 tons. The inner cover plate, not being affixed to the extrusion container, does not move at the same rate as the container, and in effect is partially extruded against the powder, so as to raise its density to substantially 100% of theoretical.
A billet having a diameter equal to that of the extrusion container and a density of substantially 100% of theoretical may be produced by loading the container and processing it in the way above set out but extruding it a distance only sufficient to accommodate the inner and outer covers in their extruded condition. The container is then removed without the remainder going through the die.

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patent: 4388054 (1983-06-01), Larsson

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