Magnetically soft, high saturation magnetization laminates...

Dynamic magnetic information storage or retrieval – Head – Core

Reexamination Certificate

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Reexamination Certificate

active

06778358

ABSTRACT:

TECHNICAL FIELD
The present invention relates to magnetic devices, for example electromagnetic transducers of disk or tape storage systems.
BACKGROUND OF THE INVENTION
Electromagnetic transducers such as heads for disk or tape drives commonly include Permalloy (approximately Ni
0.81
Fe
0.19
), which is formed in thin layers to create magnetic features. Permalloy is known to be magnetically “soft,” that is, to have high permeability and low coercivity, allowing structures made of Permalloy to act like good conductors of magnetic flux. For example, an inductive head may have conductive coils that induce magnetic flux in an adjacent Permalloy core, that flux employed to magnetize a portion or bit of an adjacent media. That same inductive head may read signals from the media by bringing the core near the magnetized media portion so that the flux from the media portion induces a flux in the core, the changing flux in the core inducing an electric current in the coils. Alternatively, instead of inductively sensing media fields, magnetoresistive (MR) sensors or merged heads that include MR sensors may use thinner layers of Permalloy to read signals, by sensing a change in electrical resistance of the MR sensor that is caused by the magnetic signal.
In order to store more information in smaller spaces, transducer elements have decreased in size for many years. One difficulty with this deceased size is that the amount of flux that needs to be transmitted may saturate elements such as magnetic pole layers, which becomes particularly troublesome when ends of the pole layers closest to the media, commonly termed pole tips, are saturated. Magnetic saturation in this case limits the amount of flux that is transmitted through the pole tips, limiting writing or reading of signals. Moreover, such saturation may blur that writing or reading, as the flux may be evenly dispersed over an entire pole tip instead of being focused in a corner that has relatively high flux density. For these reasons the use of high magnetic saturation materials (also known as high moment or high B
S
materials) in magnetic core elements has been known for many years to be desirable.
For instance, iron is known to have a higher magnetic moment than nickel, so increasing the proportion of iron compared to nickel generally yields a higher moment alloy. Iron, however, is also more corrosive than nickel, which imposes a limit to the concentration of iron that is feasible for many applications. Also, it is difficult to achieve soft magnetic properties for primarily-iron NiFe compared to primarily-nickel NiFe. Anderson et al., in U.S. Pat. No. 4,589,042, teach the use of high moment Ni
0.45
Fe
0.55
for pole tips. Anderson et al. do not use Ni
0.45
Fe
0.55
throughout the core due to problems with permeability of that material, which Anderson et al. suggest is due to relatively high magnetostriction of Ni
0.45
Fe
0.55
.
As noted in U.S. Pat. No. 5,606,478 to Chen et al., the use of high moment materials has also been proposed for layers of magnetic cores located closest to a gap region separating the cores. Also noted by Chen et al. are some of the difficulties presented by these high moment materials, including challenges in forming desired elements and corrosion of the elements once formed. Chen et al. state that magnetostriction is another problem with Ni
0.45
Fe
0.55
, and teach the importance of constructing of heads having Permalloy material layers that counteract the effects of that magnetostriction. This balancing of positive and negative magnetostriction with plural NiFe alloys is also described in U.S. Pat. No. 5,874,010 to Tao et al.
Primarily iron FeCo alloys are known to have a very high saturation magnetization but also high magnetostriction that makes them unsuitable for many head applications. That is, mechanical stress during slider fabrication or use may perturb desirable magnetic domain patterns of the head.
FIG. 11
shows a B/H loop
12
of a FeCoN layer that was formed by sputtering deposition at room temperature, the layer having a thickness of approximately 500 Å and having a composition of approximately Fe
0.66
Co
0.28
N
0.06
. The applied H-field is shown in oersted (Oe) across the horizontal axis while the magnetization of the layer is plotted in normalized units along the vertical axis, with unity defined as the saturation magnetization for a given material. The FeCoN layer has a saturation magnetization (B
S
) of approximately 24.0 kilogauss and is magnetically isotropic, as shown by the single B/H loop
12
. B/H loop
12
also indicates a very high coercivity of about 80 oersted, which is unsuitable for applications requiring soft magnetic properties.
In an article entitled “Microstructures and Soft Magnetic Properties of High Saturation Magnetization Fe—Co—N alloy Thin Films,” Materials Research Society, Spring meeting, Section F, April 2000, N. X. Sun et al. report the formation of FeCoN films having high magnetic saturation but also high magnetostriction and moderate coercivity. Sun et al. also report the formation of a thin film structure in which FeCoN is grown on and capped by Permalloy, to create a sandwich structure having reduced coercivity but compressive stress. The magnetostriction of this sandwich structure, while somewhat less than that of the single film of FeCoN, may still be problematic for head applications.
SUMMARY
In accordance with the present invention a laminated structure including a first plurality of layers containing primarily iron FeCoN interleaved with a second plurality of layers containing primarily iron FeNi is disclosed. The structure has an easy axis of magnetization and a hard axis of magnetization, has a magnetic saturation of at least about twenty-three-thousand Gauss, and has a magnetic coercivity measured substantially along its hard axis of magnetization that is less than two Oersted.


REFERENCES:
patent: 4589042 (1986-05-01), Anderson et al.
patent: 5606478 (1997-02-01), Chen et al.
patent: 6118628 (2000-09-01), Sano et al.
patent: 6259583 (2001-07-01), Fontana et al.
patent: 6449122 (2002-09-01), Yazawa et al.
patent: 6490131 (2002-12-01), Sano et al.
patent: 6538845 (2003-03-01), Watanabe et al.
patent: 6541065 (2003-04-01), Sasaki et al.
patent: 6680831 (2004-01-01), Hiramoto et al.
IEEE Transactions on Magnetics article entitled “Magnetic and Structural Properties of FeCoB Thin Films”, by C. L. Platt et al., vol. 37, No. 4, Jul. 2001, pp. 2302-2304.
IEEE Transactions on Magnetics article entitled “Magnetic Properties of RF Diode Sputtered CoxFe100-xAlloy Thin Films”, by E. J. Yun et al., vol. 32, No. 5, Sep. 1996, pp. 4535-4537.
IEEE Transactions on Magnetics article entitled “Soft High Saturation Magnetization (Fe0.7Co0.3)1-xNx”, by N. X. Sun et al., vol. 36, No. 5, Sep. 2000, pp. 2506-2508.
IEEE Transactions on Magnetics article entitled “Magnetic Properties of FeCoV Film Sandwiched by Thin Soft-Magnetic Films”, by T. Nozawa et al., vol. 37, No. 4, Jul. 2001, pp. 3033-3038.
IEEE Transactions on Magnetics article entitled “High Moment FeCoNi Alloy Thin Films Fabricated by Pulsed-Current Electrodeposition”, by X. Liu et al., vol. 37, No. 4, Jul. 2001, pp. 1764-1766.
American Institute of Physics article entitled “Improvement of Soft Magnetism of Fe90Co10Sputtered Films by Addition of N and Ta”, by S. Nakagawa et al., J. Appl. Phys. 79 (8), Apr. 15, 1996, pp. 5156-5158.
Article entitled “Microstructures and Soft Magnetic Properties of High Saturation Magnetization Fe-Co-N Alloy Thin Films”, by N. X. Sun et al., 12 pages, Apr. 2000.

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