Lyophilization process for preparing composite particles for use

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204 2, 3461351, 427123, 427124, 427125, 427146, 427152, 427202, 427203, 427205, 427220, 427221, 427350, 427377, 4273981, 4273984, 428339, 428403, 428407, 428408, 428688, 428913, B32B 516, B41C 308, B41M 500, G03G 500, G03G 502

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044541945

ABSTRACT:
A method for the preparation of conductive graphite particles useful as an electrically anisotropic support layer for an electroconductive transfer film comprising initially grinding a slurry of graphite particles in the presence of water or a solvent having freezing and vapor pressure properties similar to water, for a period of time sufficient to substantially completely disperse the graphite particles in the water or solvent. A binding or film forming polymer is then added to the graphite slurry, said polymer being soluble in the water or solvent. The resulting slurry is then subjected to a freeze drying step so that the water or solvent present is caused to sublime resulting in the formation of polymeric coated graphite particles of at least 0.2 microns in diameter. These particles can be incorporated into the support layer of a electroconductive transfer film.

REFERENCES:
patent: 4163075 (1979-07-01), Nakano et al.

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