Lower-energy process for preparing passivated inorganic...

Drug – bio-affecting and body treating compositions – Topical sun or radiation screening – or tanning preparations

Reexamination Certificate

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C523S212000, C523S216000, C524S497000, C428S530000

Reexamination Certificate

active

11135584

ABSTRACT:
The disclosure is directed to a method for reducing the chemical activity and photo activity of titanium dioxide nanoparticles comprising adding an amorphous alumina-stabilizing agent, specifically an anion, such as citric acid, to an aqueous slurry of the titanium dioxide nanoparticles; treating the aqueous slurry with a source of alumina, such as a solution of sodium aluminate, to form alumina-treated titanium dioxide nanoparticles; recovering the alumina-treated inorganic nanoparticles, wherein the nanoparticles have a particle size of about 50 to about 300 nm; and milling the nanoparticles to form nanoparticles having a particle size about 15% smaller than silica-treated inorganic nanoparticles milled under similar conditions. The titanium dioxide nanoparticles described herein are useful in cosmetic, coating and thermoplastic compositions.

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