Lower alkylene oxide purification

Distillation: processes – separatory – Adding material to distilland except water or steam per se – Organic compound

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203 70, 203 75, 203 80, 203DIG19, 549541, B01D 340, C07D30132

Patent

active

051338394

ABSTRACT:
The present invention provides an improved process for the separation of impurities from a lower alkylene oxide, such as propylene oxide, by a process wherein the impure propylene oxide is first fractionally distilled to separate higher and lower boiling impurities, then the partially purified alkylene oxide is subjected to extractive distillation to separate additional impurities, the purified propylene oxide being separated as an overhead fraction.

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patent: 3843488 (1974-10-01), Schmidt et al.
patent: 3881996 (1975-05-01), Schmidt
patent: 4402794 (1983-09-01), Nemet-Mavrodin et al.
patent: 5000825 (1991-03-01), Shih

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