Low pressure chemical vapor deposition of silicon nitride films

Coating processes – Electrical product produced – Integrated circuit – printed circuit – or circuit board

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148187, 156653, 156657, 1566591, 427 95, 4272551, 427294, B05D 512, H01L 744, B44C 122, C03C 1500

Patent

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043954383

ABSTRACT:
A process for forming a silicon nitride layer on a semiconductor wafer in a low pressure chemical vapor deposition process. The wafer is disposed in a closed reaction chamber evacuated to a low pressure and heated to an elevated temperature in the range of about 650 to 900 degrees Centigrade. The interior of the chamber is supplied with a gaseous mixture of ammonia and a silicon compound adapted to react together with the ammonia at the elevated temperature to deposit a layer of silicon nitride on the wafer. The ammonia and the selected silicon compound have a ratio of relative concentrations in the mixture which is preselected to be in the range of 4:1 and 20:1. The silicon compound may be silane, dichlorosilane, or tetrachlorosilane. Using dichlorosilane, the preferred ratio of relative concentrations of ammonia and dichlorosilane is in the range of about 6:1 to 8:1.

REFERENCES:
patent: 3549411 (1970-12-01), Bean et al.
patent: 4111724 (1978-09-01), Ogiue et al.
patent: 4279947 (1981-07-01), Goldman et al.

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