Low loss chalcogenide glass and process for making same...

Glass manufacturing – Processes of manufacturing fibers – filaments – or preforms – Process of manufacturing optical fibers – waveguides – or...

Reexamination Certificate

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C065S033100, C065SDIG015, C423S088000, C423S565000, C117S073000, C117S077000, C501S040000

Reexamination Certificate

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07418835

ABSTRACT:
This invention pertains to a chalcogenide glass of low optical loss that can be on the order of 30 dB/km or lower, and to a process for preparing the chalcogenide glass. The process includes the steps of optionally preparing arsenic monochalcogenide precursor or the precursor can be provided beforehand; dynamically distilling the precursor in an open system under vacuum from a hot section to a cold section to purify same; homogenizing the precursor in a closed system so that it is of a uniform color; disposing the distilled or purified precursor and at least one chalcogenide element at a hot section of an open distillation system; dynamically distilling under vacuum in an open system so that the precursor and the at least one chalcogenide element are deposited at a cold section of the open system in a more purified state; homogenizing the precursor and the at least chalcogenide element in a closed system while converting the precursor and the at least one chalcogenide element from crystalline phase to glassy phase.

REFERENCES:
patent: 2804378 (1957-08-01), Upton
patent: 2886495 (1959-05-01), Jerger, Jr.
patent: 2999027 (1961-09-01), Jerger, Jr.
patent: 3042501 (1962-07-01), Noblitt
patent: 3209641 (1965-10-01), Upton
patent: 1 721 997 (1996-06-01), None
Churbanov, M. F., Scripachev, I. V., Snopatin, G. E., Shiryaev, V. S., Plotnichenko, V. G., “High-Purity Glasses Based on Arsenic Chalcogenides”, Journal of Optoelectronics and Advanced materials vol. 3, No. 2, Jun. 2001, p. 341-349.
“Vacuum Distillation”, (http://en.wikipedia.org/wiki/Vacuum—distillation) accessed Jan. 11, 2007.

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