Lithium and vanadium oxide, a preparation method thereof and...

Chemistry: electrical current producing apparatus – product – and – Current producing cell – elements – subcombinations and... – Electrode

Reexamination Certificate

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C429S232000, C429S217000, C429S231950, C423S594170, C423S641000

Reexamination Certificate

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07396614

ABSTRACT:
A lithium and vanadium oxide is described having the formula Li1+xV3O8, wherein 0.1≦×≦0.25. The oxide has a monoclinic crystalline structure and comprises non-agglomerated grains in the form of monocrystalline pellets having a length L of between 1 and 100 μm, a width W such that 4<L/W<100, and a thickness t such that 4 L/t<100, with t<W, the elongation axis of the pellets being axis b of the monoclinic cell. The oxide may be prepared by mixing the Li and V precursors, without grinding or compression, heating said mixture to 565° C.-585° C. and de-agglomerating the product obtained. The oxide is suitable for use as an active material for the positive electrode of a lithium battery.

REFERENCES:
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patent: 10-116628 (1998-05-01), None
patent: WO 00/44673 (2000-08-01), None
Zhang et al., “Spectroscopic investigation of Li1+xV3O8,” Electrochimica ACTA, Elsevier Science Publishers, Barking, GB, vol. 43, No. 8, pp. 861-868, 1998.
Panero et al., “Rechargeable Li/Li1+xV3O8Cells,” Journal of the Electrochemical Society , pp. 1225-1227, May 1983.
DePicciotto et al., “Structural characterization of Li1+xV3O8insertion electrodes by single-crystal X-ray diffraction”; Solid State Ionics 62, pp. 297-307, 1993.
Benedek et al., “Structure and electrochemical potential simulation for the cathode material Li1+xV3O8”, Chemical Abstracts Service, Columbus, Ohio, US; XP002206060, 1998.
Search Report issued in International Application No. PCT/FR02/03424.

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