Lithium amide process

Details Lithium amide process Lithium amide process

1994-04-25

1996-01-23

Langel, Wayne

Chemistry of inorganic compounds

Nitrogen or compound thereof

Hydrogen containing

C01B 2100

Patent

active

054863430

ABSTRACT:
A process for the preparation of lithium amide comprising essentially forming lithium bronze by introducing at least 1 equivalent of anhydrous ammonia over a 1 to 5 hour period into a dispersion containing one equivalent of lithium in a liquid hydrocarbon solvent at a temperature of up to 40.degree. C., then after the lithium bronze is formed, heating the reaction mixture to 50.degree. to 80.degree. C. for 2 to four hours to decompose the lithium bronze and form a suspension of lithium amide in the solvent from which suspension the lithium amide is recovered.

REFERENCES:
patent: 2612436 (1952-09-01), Overhoff et al.
patent: 3542512 (1970-11-01), Honeycutt
patent: 4206191 (1980-06-01), Morrison et al.

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