Lignosulfonate additive-containing carbon black compositions

Compositions: coating or plastic – Coating or plastic compositions – Cellulose liberation waste liquor – solid – or reaction...

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530501, C08L 9702

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active

048925870

ABSTRACT:
A carbon black composition comprising carbon black and a lignin dispersant prepared by the steps of methylolating a lignin compound by reaction of less than about 2 moles formaldehyde per 1,000 grams of the lignin, and sulfonating the methylolated lignin by reaction from about 2.5 to 3.5 moles of the sulfite or bisulfite compound per 1,000 grams of lignin at an initial reaction pH of below about 6.6 and at a temperature of at least about 170.degree. C., while allowing the pH of the reaction mixture to rise to a final pH of greater than 7.5 to sequentially sulfomethylate the aromatic nucleus and sulfonate the side chain of the lignin.

REFERENCES:
patent: 2525433 (1950-10-01), Voet
patent: 4590262 (1986-05-01), Dilling

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