Leak detection using chemical markers

Chemistry: analytical and immunological testing – Process or composition for determination of physical state... – Leak detection

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44328, 44600, 44903, 261157, 261158, 261159, 250301, G01N 3100

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active

057598576

ABSTRACT:
Leakage in a heat exchanger between two liquids which are in indirect heat exchange relationship is detected by marking one of the two liquids with a colorless chemical marker and detecting it in the second liquid by extraction and conversion to a colored material. The heat exchanger liquids are preferably organic liquids which are immiscible with water. The marker is detected in a heat exchanger liquid by extraction of the marker followed by chemical conversion of the marker to a colored material that can be detected visually. Aminoalkylnaphthalenes are suitable markers which can be extracted by an acidic aqueous solution and converted to a colored material by reaction with a diazotized aromatic amine. Phenylazoalkylphenol derivatives are also suitable markers which can be extracted and simultaneously converted to a colored material with a detection reagent which is comprised of water and a water-soluble amine.

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"Detecting Leaks in Hydrotreater Feed/Effluent Heat Exchangers Using Gasoline Dyes," Mar. 1982, American Cyanamid Company, Chemical Products Division, Worldwide Catalyst Department, Wayne, New Jersey 07470.

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