Layered lithium-nickel-based compound oxide powder and its...

Chemistry: electrical current producing apparatus – product – and – Current producing cell – elements – subcombinations and... – Electrode or plural tablets – pellets or discs

Reexamination Certificate

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Details

C429S209000, C429S199000, C429S223000, C429S224000, C429S231950

Reexamination Certificate

active

11032113

ABSTRACT:
A layered lithium-nickel-based compound oxide powder for a positive electrode material for a high density lithium secondary cell, capable of providing a lithium secondary cell having a high capacity and excellent in the rate characteristics also, is provided.A layered lithium-nickel-based compound oxide powder for a positive electrode material for a lithium secondary cell, characterized in that the bulk density is at least 2.0 g/cc, the average primary particle size B is from 0.1 to 1 μm, the median diameter A of the secondary particles is from 9 to 20 μm, and the ratio A/B of the median diameter A of the secondary particles to the average primary particle size B, is within a range of from 10 to 200. In production of a layered lithium-nickel-based compound oxide powder, which comprises spray drying a slurry having a nickel compound and a transition metal element compound capable of substituting lithium other than nickel, dispersed in a liquid medium, followed by mixing with a lithium compound, and firing the mixture, the spray drying is carried out under conditions of 0.4≦G/S≦4 and G/S≦0.0012V, when the slurry viscosity at the time of the spray drying is represented by V (cp), the slurry supply amount is represented by S (g/min) and the gas supply amount is represented by G (L/min).

REFERENCES:
patent: 2004/0076882 (2004-04-01), Hosoya et al.
patent: 2005/0158546 (2005-07-01), Shizuka
patent: 10-69910 (1998-03-01), None
patent: 10-134811 (1998-05-01), None
patent: 11162466 (1999-06-01), None
patent: 11-246225 (1999-09-01), None
patent: 2003-89526 (2003-03-01), None
patent: 2003-95659 (2003-04-01), None
patent: 03/063275 (2003-07-01), None
Office Action in Chinese Application 200480000392.6 with partial English translation.
U.S. Appl. No. 10/591,911, Sep. 7, 2006, Shizuka et al.

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